Makale detayı · 2014
Synthesis Characterization Crystal Structure Thermal Behavior and Biological Activity of a New Heterotrinuclear Complex NiL NCS H2O 2Cd DMF 2
Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry
- Yıl
- 2014
- ISSN
1553-3174- Tür
- article
Veri kaynağı ayrımı
- YÖKSİS YÖKSİS makale kaydı
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Özet
İngilizce (OpenAlex)
A new trinuclear heterometallic nickel(II)-cadmium(II)-nickel(II) complex, [(NiL(NCS)(H2O))2Cd(DMF)2] (DMF: dimethylformamide) (1), has been synthesized by using NiL as the so-called metallo ligand where H2L = N,N′-bis(salicylidene)-1,3-diaminopropane, cadmium nitrate, and amonium thiocyanate. The title complex was characterized by various methods including elemental analyses, IR, 1H-NMR, 13C-NMR, TG-DTA, and X-ray diffraction techniques. The complex crystallizes in monoclinic space group P21/c, with unit cell dimensions a = 10.6217(3), b = 13.3487(4), c = 16.0043(4) Å, β = 93.823(2)°. The complex was screened for antimicrobial activities by the disc diffusion using DMF as solvent. The minimum inhibitory concentration values were calculated.
Konular
- Metal complexes synthesis and properties
- Magnetism in coordination complexes
- Metal-Organic Frameworks: Synthesis and Applications
Birincil konu Metal complexes synthesis and properties