Makale detayı · 2006 · article
Inexpensive One Pot Synthesis of Unsymmetrical Disulfides Using 1 Chlorobenzotriazole
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- YÖKSİSYÖKSİS makale kaydı
- YÖKSİS dergi adıThe Journal of Organic Chemistry
- Katalog eşleşmesi (ISSN)Journal of Organic Chemistry
- OpenAlexOpenAlex zenginleştirmesi (özet, atıf, konular)
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Özet
A new synthesis of unsymmetrical disulfides is described. The reaction of a thiol R1SH with 1-chlorobenzotriazole (BtCl) at -78 degrees C in DCM affords a high-yielding conversion to R1SBt without appreciable formation of the symmetrical disulfide R1SSR1. R1SBt is then reacted with R2SH to form the unsymmetrical disulfide in a one-pot sequence with green character that avoids the use of toxic and harsh oxidizing agents. The methodology has been developed for synthesis of various types of disulfides.
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