Makale detayı · 2013 · article
Crystal structure of bis isothiocyanato 2 6 diacetylpyridine bis 4 hydroxybenzoylhydrazone Fe III Chloride bis dimethylformamide solvate
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- YÖKSİSYÖKSİS makale kaydı
- YÖKSİS dergi adıCrystallography Reports
- Katalog eşleşmesi (ISSN)Crystallography Reports
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Özet
The crystal structure of title compound (Fe[(C 25 H 21 N 7 O 4 S 2 )] · 4(C 3 NOH 7 ), where C 3 NOH 7 is dimethylformamide, DMF) was determined by the X-ray diffraction method. This compound crystallizes in the monoclinic C2/c space group, Z = 4. Unit cell parameters are: a = 13.6080(5), b = 17.6375(7), c = 19.5571(6) Å, β = 108.753(2)°. The N-H...O and O-H...O interactions stabilize the molecules in the lattice. The structure contains also the solvent dimethylformamide molecules, which are connected with intermoleculer hydrogen bond. The O atoms of DMF molecules take place as acceptor atoms.
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